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Why am I so fucking shit at kitchen chemistry by WIAKR+Pa !1CreRGKd/6!!TfPvomrn - Thu, 07 Jul 2016 21:22:03 EST ID:5Pw/LIPu No.78073 Ignore Report Reply Quick Reply
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I fucking hate my life. Bombastus, can I please come live with you since you're actually good at chemistry? I promise I will be a faithful lab assistant, am totally willing to get a Canadian visa, and would love to learn all about how to not suck dick at kitchen chemistry.

I really need general tips on how to actually manage to perform kitchen chemistry and not fail at things as simple as fucking morphine extractions. Nothing I attempt ever seems to work. I'm just quite unhappy right now. Pls gib advice.

Sorry for the super low-res photo
4 posts omitted. Click Reply to view.
Bombastus !RZEwn1AX62!!xXxJO70U - Mon, 08 Aug 2016 00:35:51 EST ID:HCt0W/hp No.78138 Ignore Report Quick Reply
how tf did you get a rotovap. which state are you in!? wowza.

Alright, well if you have that much money, you might as well extract all your seeds with a slightly acidic solution, rinse with hexanes, basify with CaOH and NHx, and filter that off. This way, you're working with all liquids and the rotovap makes everything much easier. The washing of the seeds will be the hardest part.

Please don't go and die on me.
Press - Mon, 08 Aug 2016 07:00:50 EST ID:xrIpEC8o No.78139 Ignore Report Quick Reply
What are the petri dishes for?

Morphine is a salt at pH!=8,99 or something.
And even at the isoelectric point its a bitch to liquid-liquid extract.
Dont worry about the layers, those are just precipitation, a coarse filtration will do the same job-itll actually be a bit more efficient- if its followed by a finer filtration
Bombastus !RZEwn1AX62!!xXxJO70U - Mon, 08 Aug 2016 14:46:39 EST ID:HCt0W/hp No.78140 Ignore Report Quick Reply
Good watch glasses and lab covers.
Liquid liquid extract everything else. Then filter extract morphine. That sounds easier than other options.

HCN my shit up fam.
Press - Tue, 09 Aug 2016 03:06:51 EST ID:MKujOXWI No.78143 Ignore Report Quick Reply
Meh, shits gonna get stuck at the rims.

Just methylmercury my fam, fuck
Bombastus !RZEwn1AX62!!xXxJO70U - Tue, 09 Aug 2016 19:42:54 EST ID:HCt0W/hp No.78144 Ignore Report Quick Reply
Methylmercury is probably a great way to suicide. It's like condensed cancer and the doctors would probably give you all the opiates you want. Maybe even some benzos.

pic related of my script

How water goes up straws by James Dinningbanks - Sun, 07 Aug 2016 22:02:44 EST ID:MVUX73Om No.78135 Ignore Report Reply Quick Reply
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The reason that liquids go up straws is not because you're sucking it in but because you're displacing the oxygen inside the straw allowing the liquid to shape without the pressure of oxygen.
Bombastus !RZEwn1AX62!!xXxJO70U - Sun, 07 Aug 2016 23:32:27 EST ID:HCt0W/hp No.78136 Ignore Report Quick Reply
>displacing the oxygen
You mean the air? Specify. We're on /chem/ afteral
>allowing the liquid to shape
The definition of a liquid is that it has no shape nor does it retain on. what do you mean "the pressure of oxygen"?

Also, why did you start this thread even.
James Dinningbanks - Sun, 07 Aug 2016 23:59:23 EST ID:MVUX73Om No.78137 Ignore Report Quick Reply
I don't know, I like pretending like I know science
Bombastus !RZEwn1AX62!!xXxJO70U - Mon, 08 Aug 2016 14:47:21 EST ID:HCt0W/hp No.78141 Ignore Report Quick Reply
Good for you for admitting it, at least.


Oxymorphinol and Hydromorphinol by Bombastus !RZEwn1AX62!!xXxJO70U - Mon, 27 Jun 2016 02:29:51 EST ID:G8mu3scS No.78032 Ignore Report Reply Quick Reply
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Hey faggotqueers. Are these the same fucking thing?

Possible synthesis discussion below.
9 posts and 2 images omitted. Click Reply to view.
Press !QUHukXEvkY - Thu, 30 Jun 2016 01:16:05 EST ID:JUzW0CgK No.78046 Ignore Report Quick Reply
J. Magano, M. H. Chen, J. D. Clark, T. Nussbaumer, J. Org. Chem., 2006, 71, 7103-7105.
Bombastus !RZEwn1AX62!!xXxJO70U - Thu, 30 Jun 2016 20:27:42 EST ID:4ppVjZXo No.78047 Ignore Report Quick Reply
propanethiol and butanethiol can be smelled when in its airtight glass bottle, vacuum sealed-foil lined bag, inside of a ziplock bag coated with chemical absorbant, all while sealed in a stainless steel can. as you surpass these layers of protection, the smell gets worse and worse.
A reflux condenser is absolute suicide.
humans can smell ethanethiol at concentrations of 4ppb. i think i had propanethiol at at least 500ppm when i opened it to the atomosphere

eu not that bad. go to UK and buy a bunch of dihydrocodeine or regular codeine pills. or get someone else to do it. iunno. that seems legal. call them herbal supplemtns or calcium pills or some fucking shit

that looks promising, actually. i'll take an extra look into J. Magano et al.'s usage of 2-(Diethylamino)ethanethiol. that looks much better and more stable than fucking propane-fucking-thiol. thank god the thiols aren't toxic.
Bombastus !RZEwn1AX62!!xXxJO70U - Fri, 22 Jul 2016 21:26:14 EST ID:ycAJxrEI No.78108 Ignore Report Quick Reply
I swear these shits are the same fucking thing.
Press !QUHukXEvkY - Sun, 24 Jul 2016 04:37:05 EST ID:YPH/mOya No.78109 Ignore Report Quick Reply
You mean in their effects?
Bombastus !RZEwn1AX62!!xXxJO70U - Sun, 24 Jul 2016 14:17:21 EST ID:HCt0W/hp No.78111 Ignore Report Quick Reply
No in the molecule. I still can't see the difference and it's NOT in chirality.

microscopic telescope by Eugene Deddleham - Fri, 22 Jul 2016 13:12:29 EST ID:6cilZam8 No.78106 Ignore Report Reply Quick Reply
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I just wondered, I have never heard of a microscopic telescope. By this I mean a device along the lines of a large nature-style camera lens or traditional telecope that is able to zoom in to the target area of a physical item and produce a 3d environment of that area through the lens? Surely theres an infinite amount of detail from a physical item We have all this advanced astronomical technology these days to look at things that lie in the distance. What would happen if technology was put into microscopic telecopes thanks everyone

TLDR: a lens of intricately layered magnifying glasses that self multiply
Bombastus !RZEwn1AX62!!xXxJO70U - Fri, 22 Jul 2016 15:51:09 EST ID:ElYFdcKO No.78107 Ignore Report Quick Reply
the width of photons and their wave functions still have a measurement and you need to capture a lot of them to concentrate them. this is why a microscopic telescope isn't worth producing because they'd be so damn sensitive, there'd be no point. the curvature of the glass is also then limited due to the angles possible when the radius is limited.

Demethylation - pyridinium pathway by Bombastus !RZEwn1AX62!!xXxJO70U - Sun, 26 Jun 2016 14:02:33 EST ID:LtWIDIP2 No.78028 Ignore Report Reply Quick Reply
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Trying 3-4 different demethylation strategies under mild conditions, it seems that pyridinium HX is going to the be easiest and most non-retarded way of demethylating any species.
Any other format either seems to cleave the ether bridge, require too much heat, or is simply impractically tender.

So I wonder - does anyone have any resources on a better yielding demethylation of aromatic methoxides with pyridinium salts? Can anyone find any literature that says PyHBr would be more selective and cleaner than PyHCl with a 15% yield in demethylation of "certain" compounds? Would they be more selective or would it just not matter?

Pic unrelated
8 posts and 3 images omitted. Click Reply to view.
Bombastus !RZEwn1AX62!!xXxJO70U - Tue, 12 Jul 2016 15:57:02 EST ID:G8mu3scS No.78085 Ignore Report Quick Reply
chemical castration

also because if you can use hbr pyridine to demethylate with a higher yield, it would prove my hypothesis. it's more for science. However, i believe the pyridine has such a low yield due to the high temperatures that the reaction opeates on. 180 burns enough morphinan structures to fuck your shit up fam
do you suppose you could put it under a full vacuum and then heat it up in order to run the pyridine at a lower temperature? can you even use a solvent for the pyridine? if not, then HBr would increase its boiling point and make the decomposition even worse.
press !QUHukXEvkY - Thu, 14 Jul 2016 09:45:19 EST ID:fcMijPsC No.78086 Ignore Report Quick Reply
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well thats good! if you think that you can get enough starting material to invest your theory thatd definetely be the way to go. keep us up to date!

speaking of methyl ethers, i recently came across potassium methanolate and was wondering if it could be used to convert aryl halides to methyl ethers of aromatics. a superficial search didnt reveal anything, id guess that its a bit more hazordous to handle *i dont know* and perhaps a bit too basic to use in the presence of aldehyde groups while in higher concentrations, but whats your take on it?

ive been meaning to restart the mescaline thread with a drawn out compilation of a routes mentioned therein.
Bombastus !RZEwn1AX62!!xXxJO70U - Thu, 14 Jul 2016 13:50:50 EST ID:II1FH3AD No.78091 Ignore Report Quick Reply
don't retard the thread I'd just start a new one because that one has so much information to sift through its not worth rebumpin at this point (sorry fiend)

think I'm too busy to try this demeth though. I like science and shit but I also like my time more
press !QUHukXEvkY - Thu, 14 Jul 2016 23:57:40 EST ID:fcMijPsC No.78093 Ignore Report Quick Reply
it already was retarded the minute it started. but i agree with it being too flooded, hence i want to make a simple compilation

what about the potassium methoxide?
Bombastus !RZEwn1AX62!!xXxJO70U - Thu, 21 Jul 2016 19:25:38 EST ID:vbS8CtHn No.78105 Ignore Report Quick Reply
you'll never make a simple compilation because of the retardation that comes with being 420chan. that's just how life goes and i'm ready to fucking kill myself.

what ABOUT methoxide? i feel like that would be too strong of an electrophile and might just rip the ether open.

Is it possible to make shakenbake with lorantadine10mg/ psuedophedrine by Sidney Bottingwat - Thu, 14 Jul 2016 13:31:03 EST ID:sM4N11VN No.78087 Ignore Report Reply Quick Reply
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SWIM (someone who isn't me) wants to know if it is possible to make shakeNbake with psuedophedrine aulfate 240mg/loratadine(claritin D behind the counter)
If so, how would you do it, anons?
3 posts and 1 images omitted. Click Reply to view.
Sidney Bottingwat - Thu, 14 Jul 2016 13:54:37 EST ID:sM4N11VN No.78092 Ignore Report Quick Reply
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Eh it's out of respect. Honestly it was my dipshit friend. I know that its acetone, lithium (battery acid), draino, denatured alcohol, and sudafed but I don't want him to try it without knowing what would happen with the loratadine10mg that is per tab
Vehk !7HYGxe5v5c - Mon, 18 Jul 2016 05:23:28 EST ID:0du+stps No.78098 Ignore Report Quick Reply
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From the ingredients you're describing, I assume he is doing a birch reduction. I don't know if loratadine would react, but Sudafed as far as I'm aware is readily available in formulations which do not contain loratadine in most places.
Bombastus !RZEwn1AX62!!xXxJO70U - Mon, 18 Jul 2016 13:13:27 EST ID:AoI9o4UM No.78099 Ignore Report Quick Reply
Oh. That's what people are shake and baking now? Fucking weird.
Lorentadine shouldn't iinterfere. But I would also watch the dosage after the fact, though.
press !QUHukXEvkY - Mon, 18 Jul 2016 13:44:22 EST ID:fcMijPsC No.78100 Ignore Report Quick Reply
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my cats friends mother thinks SWIY is missing some friends of chemicals for that reaction that isnt your friends mothers reaction of something that isnt methamphetamine. maybe you should buy her some cold packs
Bombastus !RZEwn1AX62!!xXxJO70U - Thu, 21 Jul 2016 19:17:33 EST ID:vbS8CtHn No.78102 Ignore Report Quick Reply

amphetamine related by Ebenezer Snodhood - Sat, 25 Jun 2016 15:37:35 EST ID:/F1T+Pgt No.78014 Ignore Report Reply Quick Reply
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Hello guys I've been trying to reduce the P2NP (phenyl-2-nitropropene) to the amine form (amphetamine)

I tried the amalgam procedure described in erowid but this doesn't reduce the double bond (despite the rodium's archives where some people tried this and said it worked I was suspicious and tried it anyway but it doesn't give a single thing) with the "Reduction of unsubstituted P2NP by HyperLab Bee #2."

What would be a good method? LiAlH4 is expensive and difficult to handle, same with palladium or platinum compounds

I was thinking on NaBH4 to reduce the double bond and then Zn/HCl for the nitro group but I'm not sure

thanks a lot
9 posts and 3 images omitted. Click Reply to view.
Phoebe Saggledock - Sun, 03 Jul 2016 13:31:41 EST ID:JyGokHy9 No.78064 Ignore Report Quick Reply
I'll see it if
>>78062 doesn't work
Bombastus !RZEwn1AX62!!xXxJO70U - Sun, 03 Jul 2016 14:34:47 EST ID:ElYFdcKO No.78065 Ignore Report Quick Reply
There's no reason it won't work.

It's just that us clandestine-oriented chemists (Press n' me) see a more efficient method of achieving the final product compared to the academic route. Borohydride is annoying to work with due to the formation of borates (though, easily separated by a column) and since you're producing hydrogen gas in the second step, you might as well just use it to your advantage in a hydrogenation.

The 1pot reaction also benefits in that you can reuse the palladium on carbon by a simple filtration to be used over and over again. Such is the magic of Pd/C. Buy a sacrificial silica frit so you can reuse it for Pd/C. That's what I have and it works magic.
Rebecca Diddlebick - Tue, 05 Jul 2016 18:18:55 EST ID:FgNFOc9k No.78068 Ignore Report Quick Reply
thanks for your response

maybe this is a stupid question but will the aromatic ring of P2NP get reduced too if I use Pd/C? or this could only be achieved with high pressure system
Nicholas Dundleludging - Tue, 05 Jul 2016 20:07:10 EST ID:FgNFOc9k No.78069 Ignore Report Quick Reply
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ok let me see if I get your idea:

In a proper flask I put my P2NP, Zn, HCl and (if I get) palladium black? which solvent can I use? any alcohol? heating? don't I need an H2 bomb? what about the proportions of each chemical?

after a couple of hours under stirring this rxn should be done, then I go for the filter (recover Pd) and extraction, right?

ALSO: I have PcCl2 but not sure if this would work the same as Pd/C, thoughs?

great thread btw
Bombastus !RZEwn1AX62!!xXxJO70U - Tue, 05 Jul 2016 23:27:34 EST ID:LtWIDIP2 No.78070 Ignore Report Quick Reply
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benzene will not be hydrogenated at pressures lower than 60 degree. this is due to rapid isomerization of the products and reisomerization back to the reactants.
you'll need something like 30atm and 300C in order to fully hydrogenate benzene to cyclohexane.

This may be similar to your benzylic alkene but it does not engage in the main conjugation. 3atm of pressure may be necessary for this reaction at 0C. 0C increases hydrogen solubility in water and also prevents side reactions from happening.

My idea is to stir a mixture of pd/c, nitrox, zinc, and mild hydrochloric acid in a somewhat closed system for 24hours. water should be good eough since HCl. keep it at 0degrees and run the hydrogenation for 24 hours at the pressure needed to keep the balloon inflated - as per undergraduate reactions. that creates around 3atm and allows extra pressure to leak out through the side.

you might want to do 24hours of stirring as the double bond engages in electron sharing with the aromatic ring. you would filter through a pad of celite, sand, or sacrificial frit, neutralize with baking soda, and extract with toluene, dcm, ether, etc.
Wash the organic solvent with brine, dry with magnesim sulfate, dstill off the solvent, keep it under vaccum for 12 hours or whatever, and recrystallize from ethanol IF necessary.

Amphetamine solubility by Egodeath1 - Fri, 01 Jul 2016 19:20:23 EST ID:lZft8ef9 No.78055 Ignore Report Reply Quick Reply
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Okay so i dissolved 1 gram of 2 fa 2 fluroamphwtamine in 30ml of watwr. Ny question is if I let 15ml of it evaporate will i be left with some crystal 2fa?
Clara Povingmed - Fri, 01 Jul 2016 19:54:39 EST ID:iojFxQa5 No.78056 Ignore Report Quick Reply
With the way this question is phrased, worded, and spelled, I'm not sure it even deserves a response.
Egodeath1 - Fri, 01 Jul 2016 20:22:25 EST ID:lZft8ef9 No.78057 Ignore Report Quick Reply
Agreed. Ate to many darn hallucigens
Eliza Serrydock - Tue, 05 Jul 2016 03:55:57 EST ID:Snrw7+hK No.78066 Ignore Report Quick Reply
yes you will be left with 2 grams of crystal because every time you dissolve it in water and evaporate it the amount of drug doubles
press - Tue, 05 Jul 2016 16:21:58 EST ID:fcMijPsC No.78067 Ignore Report Quick Reply
maybe. i dont know the solubility.
next time use hot water and as little as possible. then just let it slowly cool down

hacking the mind by Ernest Drodgeway - Wed, 22 Jun 2016 18:21:30 EST ID:QmmUL0gM No.77992 Ignore Report Reply Quick Reply
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you know how we can put those electrodes in the heads of animals ?
we put one in the head of a rat once and they made it move with a joystick

do you think the government would weaponize i mean we could do tigers?
if we wire them right we could keep them moving through death

in theory you could do it to humans it'd be almost like zombies
1 posts omitted. Click Reply to view.
Vehk !7HYGxe5v5c - Wed, 22 Jun 2016 18:25:09 EST ID:iwIDJAAC No.77994 Ignore Report Quick Reply


Ernest Drodgeway - Wed, 22 Jun 2016 19:18:44 EST ID:QmmUL0gM No.77995 Ignore Report Quick Reply
Bombastus !RZEwn1AX62!!xXxJO70U - Wed, 22 Jun 2016 20:34:23 EST ID:V1Ngvki3 No.77996 Ignore Report Quick Reply
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Doris Chacklechuck - Fri, 01 Jul 2016 23:41:00 EST ID:0hQQ6mKi No.78061 Ignore Report Quick Reply

CrazyFolksTribe !owU3wSU682 - Fri, 15 Jul 2016 19:24:31 EST ID:Lx7wIDRk No.78096 Ignore Report Quick Reply

Finding Job with BSc in Biochemistry by Augustus Fublingdale - Tue, 07 Jun 2016 10:45:19 EST ID:1hq57uuB No.77945 Ignore Report Reply Quick Reply
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Hello guys,

I'm 22 years old and have a BSc in Biochemistry. I was wondering if it was easy to find a Job in the U.S. only with a BSc. The reason is that I need a change in environment. I somehow have the urge to travel and live in different countries.
The industry doesn't really matter it just has to make for a living and maybe it is possible to study besides working.
I'm from switzerland if that changes anything.

SLAYER to y'all
Bombastus !RZEwn1AX62!!xXxJO70U - Thu, 09 Jun 2016 18:10:13 EST ID:vbS8CtHn No.77950 Ignore Report Quick Reply
Get a masters otherwise you'll be stuck doing menial lab tech work until you're 40 and maybe then get an exec. position if you're good with money.
Cyril Chimmlebut - Thu, 16 Jun 2016 10:46:37 EST ID:1hq57uuB No.77973 Ignore Report Quick Reply

I do want to get a masters degree but I want to do that while working part-time so that I can live on my own and be a little more independent.
Bombastus !RZEwn1AX62!!xXxJO70U - Thu, 16 Jun 2016 13:07:21 EST ID:+CUD9CML No.77974 Ignore Report Quick Reply
Some Masters can pay $20000-$25000 a year.
Find one.
Molly Pabberstane - Sat, 25 Jun 2016 00:18:13 EST ID:MS463KCQ No.78010 Ignore Report Quick Reply
If you can get accepted to a PhD. program you can usually make an annual stipend of 20-25k in exchange for teaching. Work the PhD. track towards the MSc. then leave the program with your MSc.
Bombastus !RZEwn1AX62!!xXxJO70U - Fri, 01 Jul 2016 01:43:36 EST ID:bXUlP+sg No.78050 Ignore Report Quick Reply
Both; bank loan. Or you could find a job with an undergraduate and work until you have time to return for your masters.

Alkene synthesis by Esther Snodfuck - Fri, 24 Jun 2016 13:52:08 EST ID:WznVySGw No.78005 Ignore Report Reply Quick Reply
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anyone know how to solve this question with all the organic products ?
16 posts and 11 images omitted. Click Reply to view.
Bombastus !RZEwn1AX62!!xXxJO70U - Sun, 26 Jun 2016 11:49:55 EST ID:R7YMUN76 No.78025 Ignore Report Quick Reply
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Oh Vehk and Press are buttbuddies. It's okay :3

Also, I looked up the reaction and possible transition states to make sure I'm not retarded. And no. I'm not retarded:
I'm sorry, OPee. But under the falsification principle, it seems that "the software is wrong" is the most likely answer.
You could try drawing the tertiary carbocation intermediate. But that would just be retarded to ask of you.

Why are you even doing Organic chemistry in July.
This problem - Sun, 26 Jun 2016 12:03:04 EST ID:YfyCDm6o No.78026 Ignore Report Quick Reply
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I even tried that lol still said wrong idk I gonna attempt one more time then ill post answer they said was "correct", and I got a B+ in the lab1, B+ in orgo2 and an A- in lab2, but because I got a C- in the first semester of orgo the new school I transferred too said I have to retake in the summer or no diploma, I only have 1 week left so not that bad but 2300 rip for a class I already passed
Bombastus !RZEwn1AX62!!xXxJO70U - Sun, 26 Jun 2016 13:56:28 EST ID:V/Ex51MS No.78027 Ignore Report Quick Reply
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Bump. It's been two hours. What now.

I also fucking hate when schools make you do that. Sorry OP.
This problem - Sun, 26 Jun 2016 15:29:16 EST ID:YfyCDm6o No.78030 Ignore Report Quick Reply
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Wanna see some bullshit ..... stupid software I was right all along
William Clonkinman - Sun, 26 Jun 2016 15:42:25 EST ID:IK7sy6RX No.78031 Ignore Report Quick Reply
that's that pearson bullshit online hw isn't it? That's the worst shit I've ever used, the problems are all terribly made and there's typos everywhere.

Dumb scifi question by Jarvis Drerryson - Fri, 24 Jun 2016 12:37:45 EST ID:TtNn9wfR No.78004 Ignore Report Reply Quick Reply
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So I'm dicking around with a videogame, and I had the dumb idea to make a character that's essentially a biological computer, radio controlling organic drone bodies through biological radio transmitters - basically technobabble telepathy.

Would such a thing be possible, if you had countless of hours to dick around with genes and shitloads of funding?

Also, would someone be able to jam such a biological radio signal? I mean, if you can jam real radio, or take over control of a radio signal, in real life, surely you should be able to control some biological radio controlled drone...

Also, would it be possible with only radio transmitters, or could other more exotic waves be used?

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