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Harm Reduction Notes for the COVID-19 Pandemic

MXE Synthesis

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- Sat, 13 Aug 2016 11:00:34 EST xPDjzOso No.78148
File: 1471100434384.png -(16419B / 16.03KB, 220x185) Thumbnail displayed, click image for full size. MXE Synthesis
So, theoretically speaking, how hard would it be to synthesize MXE at home assuming one had no real chemistry experience or knowledge?

I'm curious because this stuff has gone the way of quaaludes and nobody is making it anymore, and after reading /dis/ for a while I've been wondering for the past few days what would making a batch imply in terms of proficiency, equipment and reagents.
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Frederick Pennerdale - Sun, 14 Aug 2016 23:21:17 EST /pQgONyj No.78152 Reply
you really think you can just synthesize a drug with no knowledge or experience? shit while you're at it why not write a symphony or build a house?
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Lillian Billingman - Mon, 15 Aug 2016 11:22:39 EST l0J9guto No.78153 Reply
i'm not actually going to try to synthesize shit, i can barely afford buying weed at the moment, buying any sort of supplies is out of the question. That, and i don't want to get bumfucked in jail.

i'm simply curious as to what the process involves in general, and thought i'd ask here. That's all.
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Edwin Grandridge - Mon, 15 Aug 2016 21:11:11 EST /pQgONyj No.78156 Reply
>>78153

The synthesis of methoxetamine is achieved by 4 steps through simple
reactions involving an aromatic nitrile, a Grignard reagent, bromination, imine
formation through reaction with a suitable amine, followed by the application
of heat to the product to allow ring expansion of 1-[(ethylimino)(3-methoxyphenyl)methyl]-1-cyclopentanol. This process is presumably readily applicable to analogues of methoxetamine by substitution of starting aromatic nitrile and selected amine to afford the desired N-substituted derivative analogues of methoxetamine.
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Priscilla Grimlock - Wed, 17 Aug 2016 02:25:33 EST HszmnPqo No.78158 Reply
So you'd need 3-methoxybenzonitrile, cyclopentyl bromide and make a grignard from it, form the intermediate ketone, brominate it and add ethylamine to get the imine and heat? for the ring expansion, would the imine get protonated, and the five membered ring turn to a six membered ring to push the double bond electrons into the nitrogen?
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Edwin Chashcocke - Wed, 17 Aug 2016 06:11:22 EST 064o23IY No.78160 Reply
>>78158
And uh. How many of those put you on a watch list?
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Priscilla Grimlock - Wed, 17 Aug 2016 06:33:38 EST HszmnPqo No.78161 Reply
>>78160
i'm not actually wanting to do it. Am not OP and just trying to figure out how to read chemistry stuff without being retarded.
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schepperschop - Wed, 17 Aug 2016 10:08:56 EST xTIigKo1 No.78162 Reply
1471442936492.jpg -(1672564B / 1.60MB, 1944x1932) Thumbnail displayed, click image for full size.
I made this scematic, is anything like this possible to be right?
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Wesley Clommerchedging - Fri, 02 Sep 2016 06:29:58 EST BClNdd0H No.78203 Reply
>>78162
Lmao what.
Looks like this is based on a misunderstanding of the nitroaldol condensation, but it's pretty fucking hard to tell.
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Schepperschop - Sat, 10 Sep 2016 19:23:26 EST xTIigKo1 No.78227 Reply
1473549806673.jpg -(836490B / 816.88KB, 2592x1944) Thumbnail displayed, click image for full size.
DICKS EVERYWHERE
>>

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